Acetic Anhydride → HCID 19882593, compound

Participants

Reaction Steps

The product from Example 14 was treated with KOH to give the free base, then reacted with acetic anhydride affording the amide. Anal. calcd. for C14H19NO2 : C, 72.07; H, 8.21; N, 6.00. Found: C, 72.03; H,.8.25; N, 6.01. This amide was reduced using the procedure of Example 5 to give the desired compound. Anal. calcd. for C14H22ClNO: C, 65.74; H, 8.67; N, 5.48. Found: C, 65.71; H, 8.61; N, 5.47.

Provenance & Evidence