Triethylamine → 3,5-Dichloro-N-[(1,1-dimethylethyl)carbonimidoyl]benzenamine

Participants

Reaction Steps

To a solution of 21.0 g of N-t-butyl-N'-(3,5-dichlorophenyl)thiourea produced in Example A-1 in 200 ml of THF were added 21.4 g of DCC and 0.73 g of triethylamine. The mixture was refluxed for 3 hours and evaporated in vacuo. The residue was extracted with petroleum ether. The extract was evaporated in vacuo to give N-t-butyl-N'-(3,5-dichlorophenyl)carbodiimide as an oil.

Provenance & Evidence