HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 67792003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 57088708 | HCID 57088708 | — |
| Product | HCID 67792003 | HCID 67792003 | — |
Reaction Steps
(2S)-1-[3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)acryloyl]-2-ethylpiperidine (trans isomer)(2.11 g) was converted to hydrobromic acid salt in a usual manner. The crystals were recrystallized from a mixture of ethyl acetate and acetone to give yellow crystals of (2S)-1-[3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)acryloyl]-2-ethylpiperidine hydrobromide (trans isomer)(1.75 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05087629 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-6ee9f373f1cd4c699b8c684f30e0fadf |
| Source note | uspto-grants-1992_02 |