1,2-Dichlorobenzene → HCID 14579766, compound

HRID 1534205Notes

Reaction equation

HRID 1534205 reaction equation
C([O:4][C:5]1[C:10]2[C:11]([CH3:16])=[C:12]([CH2:14][CH3:15])[O:13][C:9]=2[CH:8]=[CH:7][CH:6]=1)C=C.Cl[C:18]1[CH:23]=CC=C[C:19]=1Cl>>[CH2:23]([C:6]1[CH:7]=[CH:8][C:9]2[O:13][C:12]([CH2:14][CH3:15])=[C:11]([CH3:16])[C:10]=2[C:5]=1[OH:4])[CH:18]=[CH2:19]

Participants

3

Reactant 2

HCID 72391,2-DichlorobenzeneHCID 19910733HCID 19910733, compound

Product 1

HCID 14579766HCID 14579766, compound

Procedure

A mixture of 4-allyloxy-2-ethyl-3-methylbenzofuran (1.0 g; 4.8 mmoles) and orthodichlorobenzene (40 ml) was refluxed for 4 hours. The mixture was chromatographed to obtain 1.0 g of the title compound as an oil. The oil was recrystallized from hexane.

Workup

  1. temperaturewas refluxed for 4 hours
  2. customThe mixture was chromatographed

Sources & evidence

ORD record
ord-c3b13847d2ee4db89261750b7e355169
Source dataset
uspto-grants-1992_02
Patent number
US05087638

Reaction notes

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