Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | HCID 14495798 | HCID 14495798 | — |
| Product | 124728-46-7 | HCID 14495800 | — |
Reaction Steps
3-Propyl-1,2-difluorobenzene (obtainable according to Example 2) is metalated as described in 1c). 20 g of dry ice are added slowly at -70° C. The mixture is subsequently warmed to -20° C. Customary working up gives colourless crystals, m.p. 148° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05087764 |
|---|
| Source dataset | uspto-grants-1992_02 |
|---|
| ORD ID | ord-9f3851ba02e44f6780fc7a5fec1a9e62 |
|---|
| Source note | uspto-grants-1992_02 |
|---|
