HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → 2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Hexafluorocyclobutene | HCID 12767 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether | HCID 19911061 | — |
Reaction Steps
70 g (1.23 mol) of powdered potassium hydroxide are metered into a solution of 200 g (1.23 mol) of 1,2,3,3,4,4-hexafluorocyclobutene and 90 g (1:5 mol) of isopropanol in 800 ml of diethyl ether at room temperature. The mixture is stirred for a further hour and worked up as described in Example 1. The product is then distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05087775 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-bfef5c94b8544c07810aa926c21820e5 |
| Source note | uspto-grants-1992_02 |