Dimethylformamide → HCID 86745467, compound

Participants

Reaction Steps

To the salicylic acid disulfide (3) was added DTE triethylamine at a molar ratio of 1:1:1.1. The entire solution was diluted with dried DMF to a final disulfide concentration of 0.2M. The solution was adjusted to pH 10 and argon was bubbled through the solution for 1.5 hours. The pH was then adjusted to 7. Argon was again bubbled through 3-5 minutes. The solution was capped and left stirring at 4° overnight.

Provenance & Evidence