HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzylamine → HCID 135994947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzylamine | HCID 122722 | — |
| Reactant | HCID 15079348 | HCID 15079348 | — |
| Product | HCID 135994947 | HCID 135994947 | 46% |
Reaction Steps
Using the procedure described in Example 10, p-[N-(3,4-dihydro-2-methyl-4-oxo-3-pivaloyloxymethylquinazolin-6-ylmethyl)-N-(2-acetoxyethyl)amino]benzoic acid was reacted with 3-nitrobenzylamine to give p-[N-(3,4-dihydro-2-methyl-4-oxoquinazolin-6-ylmethyl)-N-(2-hydroxyethyl)amino]-N-(3-nitrobenzyl)benzamide (containing 1 equivalent of water) in 46% yield, m.p. 230°-232° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089499 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-7323db7dd084464cb5ab862328a3e674 |
| Source note | uspto-grants-1992_02 |