HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15165789, compound → HCID 15165790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15165789 | HCID 15165789 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15165790 | HCID 15165790 | 78.4% |
Reaction Steps
By reducing 2.6 g (0.013 moles) of 2-(pyrrolidin-1-yl) carbonyl-3,3-dimethyl piperidine with 0.52 g (0.013 moles) of LiAlH4 in 100 ml of dry THF, using an alkaline work-up, 2.0 g of the title compound were obtained. The compound was sufficiently pure for the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089507 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-f787019c8cec448994bd45451c97a885 |
| Source note | uspto-grants-1992_02 |