HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15165792, compound → HCID 15165793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15165792 | HCID 15165792 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15165793 | HCID 15165793 | 81.2% |
Reaction Steps
By reducing 3.3 g (15.69 mmoles) of 2-(pyrrolidin-1-yl)carbonyl-5,5-dimethyl piperidine with 0.89 g (23.5 mmoles) of LiAlH4 in 80 ml of dry THF, using an alkaline work-up, 2.5 g of the title compound were obtained. The compound was sufficiently pure for the following step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089507 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-11730d73d6444341beeb452fd60ef55b |
| Source note | uspto-grants-1992_02 |