HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15165795, compound → HCID 15165796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15165795 | HCID 15165795 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15165796 | HCID 15165796 | 71.7% |
Reaction Steps
By reducing 5.4 g (0.027 moles) of 2-(pyrrolidin-1-yl) carbonyl-4,4-dimethyl piperidine with 1.1 g (0.027 moles) of LiAlH4 in 100 ml of dry THF, using an alkaline work-up, 3.8 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089507 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-6aa386ef23cb42d8853ef4bae1f1c724 |
| Source note | uspto-grants-1992_02 |