HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzyl alcohol → HCID 178450487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzyl alcohol | HCID 21439 | — |
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Product | HCID 178450487 | HCID 178450487 | — |
Reaction Steps
A mixture of ethyl 2-butyryl-3-ethoxyacrylate (23.5 g, 0.11 mol) and 2-aminobenzyl alcohol (12.3 g, 0.1 mol) was heated to 100° for 10 minutes, then diluted with petroleum ether. On cooling, ethyl 2-butyryl-3-(2-(hydroxymethyl)phenylamino)acrylate (24.9 g, 85%) crystallized as a mixture of E/Z isomers, and was filtered off and washed with petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089504 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-dd4bef6be23b444592b1f0cb638fd07c |
| Source note | uspto-grants-1992_02 |