HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzyl alcohol → HCID 178471917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzyl alcohol | HCID 21439 | — |
| Reactant | HCID 54219628 | HCID 54219628 | — |
| Product | HCID 178471917 | HCID 178471917 | 77% |
Reaction Steps
2-aminobenzyl alcohol (12.32 g, 0.1 mol) was dissolved in ethyl 2-isobutyryl-3-ethoxyacrylate (23.57 g, 0.11 mol) stirred for 2 hours at room temperature then warmed briefly to boiling. Cooling and trituration with petroleum ether gave ethyl 2-isobutyryl-3-(2-(hydroxymethyl)phenylamino)acrylate (22.29 g, 77%) as a mixture of E/Z isomers, m.p. 72°-84°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05089504 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-8495e6a95e9f43e3b73a981ca0d6fc52 |
| Source note | uspto-grants-1992_02 |