3-(4-Hydroxyphenyl)propionic acid → HCID 19910176, compound

HRID 1534676Notes

Reaction equation

HRID 1534676 reaction equation
[CH2:1]([Sn:5](=O)[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].[OH:11][C:12]1[CH:17]=[CH:16][C:15]([CH2:18][CH2:19][C:20]([OH:22])=[O:21])=[CH:14][CH:13]=1>>[OH:11][C:12]1[CH:13]=[CH:14][C:15]([CH2:18][CH2:19][C:20]([O-:22])=[O:21])=[CH:16][CH:17]=1.[OH:11][C:12]1[CH:13]=[CH:14][C:15]([CH2:18][CH2:19][C:20]([O-:22])=[O:21])=[CH:16][CH:17]=1.[CH2:1]([Sn+2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 103943-(4-Hydroxyphenyl)propionic acidHCID 61221Dibutyltin oxide

Product 1

HCID 19910176HCID 19910176, compound

Procedure

Following the procedure of Example 1, dibutyltin oxide was reacted with 33.2 g (0.2 mole) 3-(4-hydroxyphenyl)propionic acid to yield 56 g of dibutyltin bis[3-(4-hydroxyphenyl)propionate], a white crystalline material melting at 48°-50° C.

Sources & evidence

ORD record
ord-7dbc72f2b7e04fdd96e0117bac104460
Source dataset
uspto-grants-1992_02
Patent number
US05089645

Reaction notes

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