HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 6-(Chlorocarbonyl)naphthalen-2-yl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-(Acetyloxy)-2-naphthalenecarboxylic acid | HCID 87038 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 6-(Chlorocarbonyl)naphthalen-2-yl acetate | HCID 15724809 | — |
Reaction Steps
2.0 ml of thionyl chloride and a drop of N,N-dimethylformamide were added to 1.45 g (6.30 mM) of 6-acetoxy-2-naphthoic acid, followed by refluxing for 30 minutes under stirring. Excessive thionyl chloride was distilled off from the above mixture under reduced pressure to obtain 6-acetoxy-2-naphthoyl chloride. ##STR32##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05091109 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-85492626b61e454484586e96ec679337 |
| Source note | uspto-grants-1992_02 |