HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1535006Generated: November 2, 2026
Oxalyl chloride → 2-Chloro-2-oxoethyl hexanoate
https://huagongshe.com/reaction/1535006
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-Ketooctanoic acid | HCID 128859 | — |
| Product | 2-Chloro-2-oxoethyl hexanoate | HCID 14766559 | — |
Reaction Steps
8.7 gm (0.05 mole) of hexanoylacetic acid and 12.7 gm (0.10 mole) of oxalyl chloride were mixed together at room temperature. The reaction was heated gradually over one hour at 50-60° C. for about two hours. Excess oxalyl chloride was removed under reduced pressure to yield an oil that exhibits no --OH stretch by IR. Weight was 9.6 gm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05091560 |
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| Source dataset | uspto-grants-1992_02 |
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| ORD ID | ord-66c59644c1aa45b0a34ad3780e11adf1 |
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| Source note | uspto-grants-1992_02 |
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