HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1,3,5-Trichloro-2-(2-chloroethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(2,4,6-Trichlorophenoxy)ethan-1-ol | HCID 96343 | — |
| Catalyst | Benzyltrimethylammonium chloride | HCID 5963 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 1,3,5-Trichloro-2-(2-chloroethoxy)benzene | HCID 11276959 | — |
Reaction Steps
reacting the 2-(2,4,6-trichlorophenoxy)-ethanol with thionyl chloride in the presence of benzyltrimethyl ammonium chloride in a ration of 1:60 by weight at a temperature of from 50° C. to 80° C., in the presence of carbon tetrachloride as solvent to form 2-(2,4,6-trichlorophenoxy)-ethyl chloride; and
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05091578 |
| Source dataset | uspto-grants-1992_02 |
| ORD ID | ord-d8360a6e5e154d51982d0e6f891a1e17 |
| Source note | uspto-grants-1992_02 |