Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 1,3,5-Trichloro-2-(2-chloroethoxy)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-(2,4,6-Trichlorophenoxy)ethan-1-ol | HCID 96343 | — |
| 촉매 | Benzyltrimethylammonium chloride | HCID 5963 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 1,3,5-Trichloro-2-(2-chloroethoxy)benzene | HCID 11276959 | — |
반응 단계
reacting the 2-(2,4,6-trichlorophenoxy)-ethanol with thionyl chloride in the presence of benzyl-trimethyl ammonium chloride in a ratio of 1:60 by weight at a temperature of from 50° C. to 80° C. in the presence of carbon tetrachloride as solvent to form 2-(2,4,6-trichlorophenoxy)-ethyl chloride; and
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05091578 |
| 출처 데이터셋 | uspto-grants-1992_02 |
| ORD ID | ord-dd378f618ef64a35ba6872b404d402f1 |
| 출처 메모 | uspto-grants-1992_02 |