HRID1539

反应详情

EQUATION

反应方程式

HRID 1539 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from n-hexylphosphinic acid, n-butyl ester and paraformaldehyde according to the method described in Procedure 31. Purification by chromatography, eluting with dichloromethane containing 5% methanol, gave an oil.

WORKUP

后处理

  1. customPurification by chromatography
  2. washeluting with dichloromethane containing 5% methanol
  3. customgave an oil