HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-aminothieno[3,2-b]pyridine-2-carboxylate → Methyl thieno(3,2-b)pyridine-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-aminothieno[3,2-b]pyridine-2-carboxylate | HCID 13793447 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | Methyl thieno(3,2-b)pyridine-2-carboxylate | HCID 22047416 | — |
Reaction Steps
HPLC. Using 2.40 g (11.53 mmol) of methyl 3-aminothieno[3,2-b]pyridine-2-carboxylate and 2.54 g (36.88 mmol) of sodium nitrite, 0.12 g (5% of theory) of the desired product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07732477B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-75057d8c937947d58d861833dcc3cb50 |
| Source note | uspto-grants-2010_06 |