反应详情

9.2 g (49.05 mmol) of (2-chloro-3-nitrophenyl)methanol and 13.2 g (151.8 mmol) of activated manganese(IV) oxide in 50 ml of chloroform are heated under reflux for 20 h. The mixture is filtered through kieselguhr, concentrated and dried under high vacuum. The resulting title compound is directly reacted further.

1. temperatureunder reflux for 20 h
2. filtrationThe mixture is filtered through kieselguhr
3. concentrationconcentrated
4. customdried under high vacuum
5. customThe resulting title compound is directly reacted further