3,5-Dimethoxybenzaldehyde → Bis(3,5-dimethoxyphenyl)methanol

HRID 1548016Notes

Reaction equation

HRID 1548016 reaction equation
[Br:13][c:14]1[cH:15][c:16]([O:22][CH3:23])[cH:17][c:18]([O:20][CH3:21])[cH:19]1.[CH2:24]([Li:25])[CH2:26][CH2:27][CH3:28].[CH3:1][O:2][c:3]1[cH:4][c:5]([CH:6]=[O:7])[cH:8][c:9]([O:11][CH3:12])[cH:10]1.[O:29]1[c:30]2[cH:31][cH:32][c:33]([CH:34]([c:35]3[cH:36][c:37]([O:38][CH3:39])[cH:40][c:41]([O:42][CH3:43])[cH:44]3)[OH:45])[cH:46][c:47]2[O:48][CH2:49][CH2:50]1>>[CH3:1][O:2][c:3]1[cH:4][c:5]([CH:6]([OH:7])[c:14]2[cH:15][c:16]([O:22][CH3:23])[cH:17][c:18]([O:20][CH3:21])[cH:19]2)[cH:8][c:9]([O:11][CH3:12])[cH:10]1

Participants

5

Reactant 4

HCID 817473,5-DimethoxybenzaldehydeHCID 6391871-Bromo-3,5-dimethoxybenzeneHCID 69202534(2,3-Dihydrobenzo[1,4]dioxin-6-yl)-(3,5-dimethoxyphenyl)methanolHCID 178418339Butyllithium

Product 1

HCID 67173126Bis(3,5-dimethoxyphenyl)methanol

Sources & evidence

ORD record
ord-c9970b9887224e34835c28fbd5b024c7
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (1/10)

Reaction notes

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