HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1575999Generated: October 27, 2026
Ethyl Acetate → 3'-(Octadecylcarbamoyloxy)acrylanilide
https://huagongshe.com/reaction/1575999
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Octadecyl isocyanate | HCID 66988 | — |
| Reactant | n-(3-Hydroxyphenyl)acrylamide | HCID 275403 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 3'-(Octadecylcarbamoyloxy)acrylanilide | HCID 21512975 | — |
Reaction Steps
A reaction vessel is charged with 100 parts of ethyl acetate, 16.3 parts of 3'-hydroxyacrylanilide, 29.5 parts of octadecyl isocyanate and one part of triethylamine. The reaction mixture is heated at reflux for about 1 hour, cooled to 20°C and filtered. The solids are washed with ethyl acetate and air dried to give 40.5 parts of 3'-(octadecylcarbamoyloxy)acrylanilide, m.p. 124°-126°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03979202 |
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| Source dataset | uspto-grants-1976_09 |
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| ORD ID | ord-9baf46efd9c34029b085dac9484bcec8 |
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| Source note | uspto-grants-1976_09 |
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