HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → 4-butylamino-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | CID 14590535 | HCID 14590535 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-butylamino-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester | HCID 53782720 | — |
Reaction Steps
4-Ethoxy-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester is treated with butylamine at 90° for 1 hour. After this period the mixture is cooled, diluted with water and the white crystalline precipitate is filtered off. Recrystallization from diethyl ether yields 4-butylamino-1H-pyrazolo[3,4-b]pyridine-5-carboxylic acid ethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03979399 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-0c889dc07b0c470484e3e300fac50345 |
| Source note | uspto-grants-1976_09 |