HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone → Morpholine, 4-(1-cyclohexen-1-yl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Morpholine, 4-(1-cyclohexen-1-yl)- | HCID 69589 | 94% |
Reaction Steps
Illustratively, cyclohexanone may be reacted with morpholine by refluxing these reactants in toluene for a period of about three hours at a temperature of about 110° Centigrade (°C) to yield the preferred enamine reactant, 1-morpholino-1-cyclohexene, in a yield of about 94 percent together with water which is readily removed therefrom.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03979455 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-1305d88021f54518ba48e7a86a20a92b |
| Source note | uspto-grants-1976_09 |