Water → HCID 53844725, compound

HRID 1576149Notes

Reaction equation

HRID 1576149 reaction equation
O=[C:2]([CH3:19])[CH2:3][O:4][CH:5]1[CH2:10][CH2:9][CH:8]([C:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[O:12])[CH2:7][CH2:6]1.[CH3:20][CH:21]([NH2:29])[CH2:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.O>C1C=CC=CC=1>[CH3:20][CH:21]([NH:29][CH:2]([CH3:19])[CH2:3][O:4][CH:5]1[CH2:6][CH2:7][CH:8]([C:11]([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[O:12])[CH2:9][CH2:10]1)[CH2:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

5

Reactant 3

HCID 962WaterHCID 3007AmphetamineHCID 21514833HCID 21514833, compound

Product 1

HCID 53844725HCID 53844725, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

4-(2-oxo-propoxy)-cyclohexanophenone (0.02 mole) and α-methyl-phenethylamine (0.02 mole) are then heated in benzene solution. The water formed is removed by means of a Dean-Stark apparatus.

Workup

  1. customis removed by means of a Dean-Stark apparatus

Sources & evidence

ORD record
ord-fbb531f7342c480b85ef6e3c33486faf
Source dataset
uspto-grants-1976_09
Patent number
US03979456

Reaction notes

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