HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20312376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Trimethylhydroquinone | HCID 12785 | — |
| Reactant | Dodecylamine | HCID 13583 | — |
| Product | HCID 20312376 | HCID 20312376 | — |
Reaction Steps
A mixture of paraformaldehyde (6.0 g., 0.2 mole) and dodecylamine (18.5 g., 0.1 mole) is refluxed in ethanol until nearly everything dissolves. A solution of 15.2 g. (0.1 mole) trimethylhydroquinone in 100 ml. of ethanol is added and is refluxed for 2 hr. On cooling, the product precipitates as a fluffy white solid. The yield is 19.3 g. The NMR spectrum confirms the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03980479 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-6d18ca9e31774572ae8e76ae40361536 |
| Source note | uspto-grants-1976_09 |