HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 70635363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | HCID 178508063 | HCID 178508063 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 70635363 | HCID 70635363 | 90.2% |
Reaction Steps
5parts of 1-phenyl-4-amino-6-mercaptopyridazinium chloride in 100 parts of toluene is stirred with 2.5 parts of benzyl chloride for 1 hour at 110°C. 6.2 parts (90.2% of theory) of 1-phenyl-4-amino-6-benzylmercaptopyridazinium chloride is obtained; C17H16N3SCl, melting point 226° to 228°C after having been recrystallized from alcohol. The perchlorate melts at 170° to 171°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03980633 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-9d4e36b319c14516bc26c23a88144281 |
| Source note | uspto-grants-1976_09 |