HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 21512712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 20373084 | HCID 20373084 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21512712 | HCID 21512712 | — |
| Product | HCID 21512756 | HCID 21512756 | — |
Reaction Steps
A mixture of 2.44 g of 1-(3-chloropropyl)-2-chloromethyl-indoline, 3.2 g of benzylamine, 30 ml of acetone and 20 ml of water is boiled for 10 hours. 1-(3-Benzylaminopropyl)-2-chloromethyl-indoline and 1-(3-chloro-propyl)-2-benzylaminomethyl-indoline are formed intermediately and are not isolated. After the customary working up, 2-benzyl-2,3,4,5,11,11a-hexahydro-1H-1,4-diazepino-[1,2-a]indole is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03980797 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-c49335af589442548a6c509cab247f02 |
| Source note | uspto-grants-1976_09 |