2-Amino-5,6-dichlorobenzimidazole → HCID 86734002, compound

HRID 1576536Notes

Reaction equation

HRID 1576536 reaction equation
[NH2:1][C:2]1[NH:3][C:4]2[CH:10]=[C:9]([Cl:11])[C:8]([Cl:12])=[CH:7][C:5]=2[N:6]=1.Cl[CH2:14][S:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[Br:22]>>[Cl-:11].[NH2:1][C:2]1[N:3]([CH2:14][S:15][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[Br:22])[C:4]2[CH:10]=[C:9]([Cl:11])[C:8]([Cl:12])=[CH:7][C:5]=2[N+:6]=1[CH2:14][S:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[Br:22]

Participants

3

Reactant 2

HCID 4660162-Amino-5,6-dichlorobenzimidazoleHCID 218284941-Bromo-2-[(chloromethyl)sulfanyl]benzene

Product 1

HCID 86734002HCID 86734002, compound

Procedure

Following the procedure of Example 2 and replacing 2-aminobenzimidazole with 2-amino-5,6-dichlorobenzimidazole and replacing 2-bromo-4-chlorophenyl chloromethyl ether with 2-bromophenyl chloromethyl sulfide, the title compound is obtained.

Sources & evidence

ORD record
ord-530c67396eb44546aa86da3ba9cd5356
Source dataset
uspto-grants-1976_09
Patent number
US03981886

Reaction notes

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