HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-Acetoxy-2-(carbethoxymethyl)cyclopent-1-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | Ethyl 2-(2-oxocyclopentyl)acetate | HCID 2723663 | — |
| Product | 1-Acetoxy-2-(carbethoxymethyl)cyclopent-1-ene | HCID 20324204 | — |
Reaction Steps
In the manner described in Example 20, treatment of 2-(carbethoxymethyl)cyclopentan-1-one (Example 19) with acetic anhydride and p-toluenesulfonic acid monohydrate gives an oil, b.p. 130°-131°C. (7 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981868 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-4257ad8a283e4a9793ce5fa07e0c8dcc |
| Source note | uspto-grants-1976_09 |