HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → Propylene Glycol Diacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Phosphorus trichloride | HCID 24387 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Propylene Glycol Diacetate | HCID 12198 | — |
Reaction Steps
2 g phosphorus trichloride and 2 g phosphorus pentachloride were dissolved with 2 g cupric chloride in 500 ml glacial acetic acid and 50 ml acetic anhydride and then further treated a described in Example 4. 5.2 g propylene glycol diacetate were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981908 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-9fb393df01d74b2a9413980d2239cee6 |
| Source note | uspto-grants-1976_09 |