Cyclohexanol → HCID 178514813, compound

HRID 1576576Notes

Reaction equation

HRID 1576576 reaction equation
[O-2].C[Si](C)(C)[O:4][V+2:5]([O:11][Si](C)(C)C)O[Si](C)(C)C.Br[C:19]1[CH:24]=[CH:23][C:22]([Si](C2C=CC(Br)=CC=2)(C2C=CC(Br)=CC=2)[OH:26])=[CH:21][CH:20]=1.C1(O)CCCCC1>>[O-2:4].[CH:19]1([O:11][V+4:5])[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1.[O-2:26]

Participants

4

Reactant 3

HCID 7966CyclohexanolHCID 21494694Tris(4-bromophenyl)silanolHCID 178504322HCID 178504322, compound

Product 1

HCID 178514813HCID 178514813, compound

Procedure

tris-(trimethylsiloxy)-vanadium oxide is reacted with tri-(p-bromophenyl)-silanol and cyclohexanol in a molar ratio of 1:2:1 to produce bis-[tri-p-bromophenyl)-siloxy]-cyclohexyloxy-vanadium oxide [mol peak = 1184 ref to 79Br]; and

Sources & evidence

ORD record
ord-f82c48782ec7482badeb4368a58d6770
Source dataset
uspto-grants-1976_09
Patent number
US03981896

Reaction notes

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