HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → Squalane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Acetylene | HCID 6326 | — |
| Product | Squalane | HCID 8089 | — |
Reaction Steps
Ethynylation of 194 g of citronelliodene acetone was carried out with acetylene in the same manner as in example 20 except that citronellidene acetone was used in place of pseudoionone and 278 g of a crude product was thus obtained. This product was subjected to oxydative-coupling, hydrogenation and hydrogenolysis in sequence in the same manner as in example 20 and squalane was thus obtained in a yield of 36.3 % from citronellidene acetone to squalane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981930 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-1df100cf3da846e19b08e1147018cc11 |
| Source note | uspto-grants-1976_09 |