HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Ethyl 3-methylamino-4-cyclohexylphenylglyoxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Ethyl 3-amino-4-cyclohexylphenylglyoxylate | HCID 20515218 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Ethyl 3-methylamino-4-cyclohexylphenylglyoxylate | HCID 20515175 | — |
Reaction Steps
To a solution of 0.01 moles of ethyl 3-amino-4-cyclohexylphenylglyoxylate in 100 ml. of pyridine is added 0.1 moles of methyl iodide. The reaction mixture is stirred overnight at room temperature, filtered and concentrated. The residue is distilled to obtain ethyl 3-methylamino-4-cyclohexylphenylglyoxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03981932 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-39cfefd1bb164587a5be7dce19090792 |
| Source note | uspto-grants-1976_09 |