Phenethyl bromide → HCID 68145941, compound

HRID 1576666Notes

Reaction equation

HRID 1576666 reaction equation
[OH:1][C:2]1([C:8]2[CH:13]=[CH:12][C:11]3[O:14][CH2:15][O:16][C:10]=3[CH:9]=2)[CH2:7][CH2:6][NH:5][CH2:4][CH2:3]1.[CH2:17](Br)[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>CC(C)=O>[CH2:17]([N:5]1[CH2:6][CH2:7][C:2]([OH:1])([C:8]2[CH:13]=[CH:12][C:11]3[O:14][CH2:15][O:16][C:10]=3[CH:9]=2)[CH2:3][CH2:4]1)[CH2:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

4

Reactant 2

HCID 7666Phenethyl bromideHCID 150347154-(2H-1,3-Benzodioxol-5-yl)piperidin-4-ol

Product 1

HCID 68145941HCID 68145941, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

2.2 g. 4-Hydroxy-4-(3.4-methylene dioxy phenyl)-piperidine are dissolved hot in 35 ml. acetone, the solution is mixed with 0.95 g β phenethyl bromide and the reaction mixture is refluxed.

Workup

  1. temperaturethe reaction mixture is refluxed

Sources & evidence

ORD record
ord-33be8a2157854119b242cee3da8571a7
Source dataset
uspto-grants-1976_09
Patent number
US03982001

Reaction notes

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