4-Nitrobenzoyl chloride → HCID 21486331, compound

HRID 1576708Notes

Reaction equation

HRID 1576708 reaction equation
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=1.[N+:14]([C:17]1[CH:25]=[CH:24][C:20]([C:21](Cl)=[O:22])=[CH:19][CH:18]=1)([O-:16])=[O:15]>>[N+:14]([C:17]1[CH:18]=[CH:19][C:20]([C:21]([NH:1][C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=2)=[O:22])=[CH:24][CH:25]=1)([O-:16])=[O:15]

Participants

3

Reactant 2

HCID 85024-Nitrobenzoyl chlorideHCID 2357134-Amino-2-nitrobenzoic Acid

Product 1

HCID 21486331HCID 21486331, compound

Procedure

4-(4-Nitrobenzoylamino)-2-nitrobenzoic acid was prepared as described in Example 3 from 20.0 g (0.11 mol) of 4-amino-2-nitrobenzoic acid and 22.4 g (0.121 mol) of 4-nitrobenzoyl chloride. The product was reprecipitated from THF/H2O.

Workup

  1. customThe product was reprecipitated from THF/H2O

Sources & evidence

ORD record
ord-8d8602667b654e67ab6c04ef110121e9
Source dataset
uspto-grants-1976_09
Patent number
US03982011

Reaction notes

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