HRID1576907

反应详情

EQUATION

反应方程式

HRID 1576907 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

10.35 Parts of N-acetyl-D-phenylalanine is dissolved in 40 parts of methanol, then treated with 17.9 parts of DL-phenylalanine methyl ester. A precipitate forms immediately and an additional 60 parts of methanol is added. The mixture then is filtered and the solid remaining is washed with additional methanol and dried to yield the crude salt of N-acetyl-D-phenylalanine and L-phenylalanine methyl ester.

WORKUP

后处理

  1. filtrationThe mixture then is filtered
  2. washthe solid remaining is washed with additional methanol
  3. customdried