HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → 4-Benzyloxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-Benzyloxybenzonitrile | HCID 561371 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Benzyloxybenzamide | HCID 2726431 | — |
Reaction Steps
A mixture of 4-cyanophenoxy phenyl methane (10.45g.; 0.05 mole), 30% hydrogen peroxide (20ml) and 6N NaOH (20ml) and ethanol (30ml) was maintained at 40°-50° for 3 hrs., cooled and neutralised. The product was filtered off and recrystallised from ethanol M.p. 186°-7°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983164 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-0adf8d62de3f4a3692562c6158bddfe6 |
| Source note | uspto-grants-1976_09 |