1-Propanesulfonyl chloride → HCID 54330345, compound

Participants

Reaction Steps

Eight and one-half grams of 4-methylbenzohydroximoyl chloride, prepared as in Example VI-A, was treated with 7.1 g of propanesulfonyl chloride in the same manner as described in Example VI-B. Recrystallization of the oil from ethanol gave 8.1 g of N-(propanesulfonyloxy)-4-methylbenzimidoyl chloride, m.p. 57.5°-60.5°. The ir spectrum was consistent with the assigned structure.

Provenance & Evidence