HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21510400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21510409 | HCID 21510409 | — |
| Product | HCID 21510400 | HCID 21510400 | 77.1% |
Reaction Steps
In the same manner as described in Example 7, 2-(β-hydroxyethyl)-5,8-dimethyl-2,3,4,4a,5,9b-hexahydro-1H-pyrido-[4,3-b]indole (3.5 g) is reacted with thionyl chloride (5.0 g) to give 2-(β-chloroethyl)-5,8-dimethyl-2,3,4,4a,5,9b-hexahydro-1H-pyrido[4,3-b]indole (2.9 g) as an oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983239 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-69a48be3c60345a893d689fd25c079b8 |
| Source note | uspto-grants-1976_09 |