HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Methoxyphenyl)-1-phenylprop-2-en-1-one → 8-(4-Methoxyphenyl)-10,10-dimethyl-6-phenyl-10H-pyrido[1,2-a]indolium perchlorate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Methoxyphenyl)-1-phenylprop-2-en-1-one | HCID 94197 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl-, perchlorate | HCID 14913188 | — |
| Product | 8-(4-Methoxyphenyl)-10,10-dimethyl-6-phenyl-10H-pyrido[1,2-a]indolium perchlorate | HCID 12374370 | — |
Reaction Steps
2,3,3-Trimethyl-3H-indolium perchlorate (5 g.) and 3-(4-methoxyphenyl)-1-phenyl-prop-2-ene-1-one (10 g.) were heated together on a steam bath for three hours. The cooled mixture was purified by recrystallization from acetonitrile. The melting point is 258°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03983288 |
| Source dataset | uspto-grants-1976_09 |
| ORD ID | ord-a47521511e23444a9257f90a109acb4d |
| Source note | uspto-grants-1976_09 |