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HRID1577040

反应详情

EQUATION

反应方程式

HRID 1577040 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(C=CC(C)=O)cc1
HCID95414

3-Buten-2-one, 4-(4-methoxyphenyl)-

C11H12O2

结构：CC1=[NH+]c2ccccc2C1(C)C.[O-][Cl+3]([O-])([O-])[O-]
HCID14913188

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(-c2cc(C)[n+]3c(c2)C(C)(C)c2ccccc2-3)cc1.[O-][Cl+3]([O-])([O-])[O-]
HCID12374368

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

2,3,3-Trimethyl-3H-indolium perchlorate (5 g.) and 4-p-methoxyphenylbut-3-ene-2-one (10 g.) were heated together on the steam bath for three hours. The cooled mixture was diluted with methanol and filtered. The product was purified by recrystallization from acetonitrile. Yield 4.1 g.; m.p. 298°-300° .

WORKUP

后处理

  1. filtrationfiltered
  2. customThe product was purified by recrystallization from acetonitrile