Bromine → HCID 12557060, compound

HRID 1577061Notes

Reaction equation

HRID 1577061 reaction equation
[CH2:1]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[Br:13]Br>C(O)(=O)C>[Br:13][C:10]1[CH:11]=[C:6]([CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[CH:7]=[CH:8][C:9]=1[OH:12]

Participants

4

Reactant 2

HCID 24408BromineHCID 269754-Pentylphenol

Product 1

HCID 12557060HCID 12557060, compoundYield 89.5%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

24.6 g (0.15 mol) of p-n-pentylphenol was reacted with 24.5 g (0.153 mol) bromine in glacial acetic acid to yield 32.6 g of 2-bromo-4-n-pentylphenol by vacuum distillation or a yield of 89.5%.

Sources & evidence

ORD record
ord-627e1fb552414c81af3398e04217c36d
Source dataset
uspto-grants-1981_09
Patent number
US04287085

Reaction notes

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