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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1577330Generated: November 3, 2026

HCID 20506402, compound → HCID 20506389, compound

https://huagongshe.com/reaction/1577330

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 20506402HCID 20506402—
ReactantHCID 53720619HCID 53720619—
SolventIsoamyl AlcoholHCID 31260—
ProductHCID 20506389HCID 20506389—

Reaction Steps

A mixture of 0.1 mole of 2-methylmercapto-4-amino-6-chloro-7,8-dimethoxyquinazoline and 0.12 mole of 3-n-hexylpyrrolidine in isoamyl alcohol is heated at reflux for 16 hours, cooled, washed with water and the organic phase is concentrated in vacuo. Hexane is slowly added to the residue and the solid title compound is collected and purified, if desired by silica gel column chromatography.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04287341
Source datasetuspto-grants-1981_09
ORD IDord-bc5e449b4d454195844d81f766cf6c2e
Source noteuspto-grants-1981_09