Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N-(1-cyano-1,2-dimethylpropyl)-2,3-Dibromopropionamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2,3-Dibromopropanoyl chloride | HCID 86790 | — |
| 반응물 | 2,3-Dimethyl-2-aminobutyronitrile hydrochloride | HCID 12945444 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-(1-cyano-1,2-dimethylpropyl)-2,3-Dibromopropionamide | HCID 12945446 | — |
반응 단계
A mixture of 4.5 g (0.03 mole) of the 2,3-dimethyl-2-aminobutyronitrile hydrochloride, 4.8 g (0.06 mole) of 50% aqueous sodium hydroxide, 15 ml of dichloromethane and 15 ml of water was prepared. A second solution of 7.5 g (0.03 mole) of 2,3-dibromopropionyl chloride in 15 ml dichloromethane was added with rapid stirring to the first mixture at 10°-15° C. The mixture was then allowed to reach room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04288384 |
| 출처 데이터셋 | uspto-grants-1981_09 |
| ORD ID | ord-83032e0dcd9444a0816d283a3e1f5bfe |
| 출처 메모 | uspto-grants-1981_09 |