反应详情

51.6 g (i.e., 0.215 mol) of tris-(2-chloroethyl)-amine hydrochloride were added to the above mixture (a). The mixture was subsequently heated at the reflux temperature of the 2-methoxyethanol (125° C.) for 12 hours and the solvent was then distilled under reduced pressure. The excess sodium 2-methoxyethanolate was neutralized by adding 11.6 cm3 of aqueous HCl (10 N) thereto. The sodium chloride was filtered off and the solution was distilled.

1. distillationthe solvent was then distilled under reduced pressure
2. additionby adding 11.6 cm3 of aqueous HCl (10 N)
3. filtrationThe sodium chloride was filtered off
4. distillationthe solution was distilled