1-Methylthio-1-methylamino-2-nitroethylene → N-[2-[[5-(Dimethylaminomethyl)-4-methyl-2-furanylmethyl]thio]ethyl]-N'-methyl-2-nitro-1,1-ethenediamine

Participants

Reaction Steps

A mixture of 5-[[2-(amino)-ethyl]thio]methyl-N,N,3-trimethyl-2-furanmethanamine (1.15 g) and N-methyl-1-(methylthio)-2-nitroethenamine (0.76 g) was heated in vacuo for 4 hours. The reaction mixture was purified by column chromatography (silica/methanol:0.88 ammonia 79:1) affording the title compound (0.45 g).

Provenance & Evidence