HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 20570875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | HCID 20570870 | HCID 20570870 | — |
| Product | HCID 20570875 | HCID 20570875 | 24% |
Reaction Steps
2,3-Diamino-4,5-dimethyl-1-[2-hydroxy-3-(4-phenoxymethylpiperidino)-propoxy]-benzene trihydrochloride is reacted with phosgene analogously to Example 1 to give 4-[2-hydroxy-3-(4-phenoxymethylpiperidino)-propoxy]-6,7-dimethyl-2-benzimidazolinone hydrochloride in a yield of 24% of theory; m.p. 273°-275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288442 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-2f25fa453d824948a21aa1ecf86f3fc3 |
| Source note | uspto-grants-1981_09 |