HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178457123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- | HCID 4712192 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178457123 | HCID 178457123 | 43% |
Reaction Steps
Prepared as in Example 1 from 2-benzoyl-benzo[b]thiophen-3-ol, phosphorus(V) chloride and a solution of one part by volume of allylamine in 2 parts by volume of water with a yield of 43% of theory. M.p. 104°-106° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288437 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-1b0dab7777a145188dd7f872712b4f3f |
| Source note | uspto-grants-1981_09 |